烧结温度对Mo2FeB2高熵金属陶瓷组织与性能的影响Effect of sintering temperature on microstructure and properties of Mo2FeB2 high entropy metal ceramics
周恩瑞,潘应君,柯德庆
摘要(Abstract):
采用真空液相烧结工艺制备了Mo_2FeB_2高熵金属陶瓷材料。借助X射线衍射仪(X-ray diffraction)、扫描电镜(Scanning electron microscopy)、能谱仪(Energy dispersive spectroscopy)和洛氏硬度计分析不同烧结温度对Mo_2FeB_2高熵金属陶瓷组织与性能的影响。结果表明:Mo_2FeB_2高熵金属陶瓷由Mo_2FeB_2硬质相、Cr_(23)C_6硬质相和FeMnCrNi高熵合金粘结相构成;随着烧结温度的升高,高熵金属陶瓷的硬度和断裂韧性呈现先增加后减小趋势,当烧结温度为1260℃时达到峰值,分别为68.8 HRC和10.1 MPa·m~(1/2);FeMnCrNi高熵合金粘结相通过晶格畸变并与Mo_2FeB_2硬质相晶粒形成桥接,导致高熵金属陶瓷韧性的提高。
关键词(KeyWords): Mo_2FeB_2;高熵陶瓷;烧结温度
基金项目(Foundation): 省部共建耐火材料与冶金国家重点实验室青年基金(2018QN04)
作者(Author): 周恩瑞,潘应君,柯德庆
DOI: 10.13289/j.issn.1009-6264.2024-0258
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